Methods for Testing Free SO2 in Wine Aeration-Oxidation (AO) Method for Free SO2 This is the original primary laboratory method for sulfite measurement in wine that helps define what "free" SO2 means. In the AO method, a wine sample is placed in a flask and phosphoric acid is added to force the sulfite ion into molecular SO2.5/5(1)Missing:enervacMust include:enervacFree SO2 - Accuvin
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